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kick-off meeting of the H2020 FET OPEN project OXiNEMS

The kick-off meeting of the H2020 FET OPEN project OXiNEMS has been organized at CNR-SPIN headquarters in Genova on May 6th and 7th, 2019.

The involved European groups gathered to strengthen relationships, have scientific discussions and detail the first steps of the project.The OXiNEMS project plans to develop innovative nanoelectromechanical systems (NEMS) based on multifunctional (epitaxial) transition metal oxides. The OXiNEMS team will implement ultrasensitive detectors able to measure very weak magnetic fields targeting those generated by human brain activity, of the order of tens of femtotesla.

Our article "Magnetic Trampoline Resonators Made of (La,Sr)MnO3 Single-Crystal Thin Films" has been published on ACS Sensors!

 

Abstract: Microelectro-mechanical resonators employing a magnetic element have been proposed for magnetic field sensing applications, but the integration of magnetic materials with standard semiconductor compounds is challenging and requires complex fabrication protocols. We present a different approach relying on (La0.7,Sr0.3)MnO3 (LSMO), an oxide compound that works both as a structural element for the resonator and a functional magnetic layer. Suspended trampolines are realized in a single-step process from LSMO thin films and show a quality factor of up to 60k and f·Q products reaching 1010 Hz. Their magnetic properties are probed by a SQUID magnetometer and magnetic force microscopy, showing a saturation magnetization of 240 kA/m at room temperature and in-plane magnetic domains with a coercivity of 2.5 mT. Being entirely made from a magnetic material, these resonators exhibit a larger magnetic interaction volume compared to other solutions, making them ideal candidates as building blocks for high-sensitivity magnetic field sensors.

 

Our article "Oxide Membranes from Bulk Micro-Machining of SrTiO3 Substrates" has been accepted on Advanced Science !

 

abstract: Suspended micro-structures made of epitaxial complex oxides rely on surface micro-machining processes based on sacrificial layers. These processes prevent to physically access the microstructures from both sides, as substantial part of the substrate is not removed. In this work, a bulk micromachining protocol is developed for a commonly used substrate employed in oxide thin films deposition. Suspended oxide thin film devices are realized by fabricating pass-through holes across SrTiO3(100) or SrTiO3(110) substrates. Careful calibration of anisotropic etching rates allows controlling the final geometry of the aperture in the substrate in a predictable way. As demonstrators of possible device geometries, clamped membranes and trampolines realized from deposited thin films of (La,Sr)MnO3, a conductive magnetic oxide, and a suspended trampoline resonator carved from the SrTiO3 substrate itself are presented. Reported protocols can be readily applied to a broad variety of other complex oxides so to extend the use of membranes technology beyond those of commercially available silicon compounds.

This year the results of the OXiNEMS project have been presented at the 30th International workshop on Oxide Electronics (iWOE30) held in Darmstadt (Germany) from 29 September to 2 October 2024.

Here the list of our presentations:

  • "Bulk micro-machining of SrTiO3 substrates for device applications" (Poster by Nicola Manca)
  • "Strain, Young’s modulus, and structural transition of EuTiO3 thin films probed by micro-mechanical methods" (Poster by Daniele Marré)
  • "(La0.7,Sr0.3)MnO3 trampoline resonators for magnetometers and IR bolometers" (Poster by Luca Pellegrino)
  • …and one oral contribution “Integration of High-Tc Superconductors and High Q-factor Mechanical Resonators in LaAlO3 Suspended Micro-Bridges” given by Nicola Manca

 

Our article “Integration of High-Tc Superconductors with High-Q-Factor Oxide Mechanical Resonators” has been accepted for publication on Advanced Functional Materials."

We realized a micro-mechanical resonator showing both high mechanical Q-factor and superconductivity at 77 K. This result was achieved by integrating a high-Tc superconductor YBa2Cu3O7 (YBCO) with a high Q-factor micro-bridge resonators made of single-crystal LaAlO3 (LAO) thin films. Bare LAO resonators are tensile strained, with a stress of about 350 MPa, and show a mechanical Q-factor above 200k at room temperature. Additionally, they have low surface roughness. A YBCO film was then grown ex-situ by pulse laser deposition on top of the suspended bridges. Final devices show zero resistance below 78 K and mechanical properties similar to those of bare LAO ones. These results open new possibilities towards the development of advanced transducers, such as bolometers or magnetic field detectors, as well as experiments in solid state physics, material science, and quantum opto-mechanics.

For further readings:

N. Manca, A. Kalaboukhov, A. E. Plaza, L. Cichetto Jr., E. Wahlberg, E. Bellingeri, F. Bisio, F. Lombardi, D. Marré, L. Pellegrino, “Integration of High-Tc Superconductors with High-Q-Factor Oxide Mechanical Resonators” Adv. Funct. Mater. 2024, 2403155.

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